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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 9
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Original Articles

Expedient and High-Yield Synthesis of Alkylphos-Phonyl Bichlorides Under Mild, Neutral Conditions: Reaction of Bis(Trimethylsilyl)Alkyl Phosphonates with Oxalyl Chloride/Dimethylformamide

Nandkumar N. Bhongle Department of Medicinal Chemistry, University of Rhode Island, Kingston, Rhode Island, 02881
,
Robert H. Notter Department of Chemical Engineering, University of Rochester, Rochester, New York, 14642
&
Joseph G. Turcotte Department of Medicinal Chemistry, University of Rhode Island, Kingston, Rhode Island, 02881
Pages 1071-1076 | Published online: 19 Dec 2006
 
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Abstract

Structurally variant bis(trimethylsilyl)alkyl phosphonates were converted in high yields (80–88%, distilled) to the corresponding phosphonyl dichlor-ides upon reaction with (COCl)2/DMF.

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