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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 9
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Original Articles

Syntheses of E-2-Nitroethenyltrimethylsilane

Robert F. Cunico Department of Chemistry, Northern Illinois University, DeKalb, Illinois, 60115, USA
Pages 917-923 | Published online: 05 Dec 2006
 
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Abstract

Three routes were explored for the conversion of tri-methylvinylsilane (1) to E-2-nitroethenyltrimethylsilane (2). In each case, 2 was afforded by base-induced vicinal elimination within the adducts arising from 1 plus (a) NO2C1 (b) N2O4 or (c) HgC12 + NaNO2.

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