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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 9
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Original Articles

Efficacious Entry Into Substituted 5,6-Dihydro-4-Hydroxy-2H-Pyran-2-Ones and 2,3-Dihydro-4H-Pyran-4-Ones Utilizing Ketonic Dianions

John R. Peterson The Michael Faraday Laboratories, Department of Chemistry, Northern Illinois University, DeKalb, IL, 60115
,
Tamara J. Winter The Michael Faraday Laboratories, Department of Chemistry, Northern Illinois University, DeKalb, IL, 60115
&
Chris P. Miller The Michael Faraday Laboratories, Department of Chemistry, Northern Illinois University, DeKalb, IL, 60115
Pages 949-963 | Published online: 05 Dec 2006
 
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Abstract

Methyl acetoacetate and 2,4-pentanedione dianions were condensed with aldehydes and ketones to afford a 1,3,5-trioxygenated carboskeleton. Intramolecular cyclization of the aldol adducts delivered the title compounds in good yield.

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