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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 4
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Original Articles

Sterically-Driven Anhydride Formation

J. L. Belletire Department of Chemistry, University of Cincinnati, Cincinnati, Ohio, 45221-0172
&
G. M. Conroy Department of Chemistry, University of Cincinnati, Cincinnati, Ohio, 45221-0172
Pages 403-415 | Published online: 06 Dec 2006
 
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Abstract

Oxidative coupling of highly substituted carboxylic acid dianions affords hindered succinic acid derivatives which undergo facile intramolecular anhydride formation. A novel, but low yield, synthetic sequence converts 4′-methoxypropiophenone into diethylstilbestrol.

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