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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 13
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Original Articles

Electrochemical Synthesis of Trifluoromethane Sulfinic Acid Salt From CF3Br and SO2

Jean-Claude Folest Laboratoire d'Electrochimie, Catalyse et Synthèse Organique, U.M. 28, C.N.R.S., 2, rue Henri-Dunant, 94320, Thiais, France
,
Jean-Yves Nédélec Laboratoire d'Electrochimie, Catalyse et Synthèse Organique, U.M. 28, C.N.R.S., 2, rue Henri-Dunant, 94320, Thiais, France
&
Jacques Périchon Laboratoire d'Electrochimie, Catalyse et Synthèse Organique, U.M. 28, C.N.R.S., 2, rue Henri-Dunant, 94320, Thiais, France
Pages 1491-1494 | Published online: 03 Jan 2007
 
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Abstract

The electroreduction of a mixture of SO2 and CF3Br in DMF, in an undivided cell with a soluble anode (Mg or Zn) lead to salt of trifluoromethane sulfinic acid in high yield.

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