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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 18, 1988 - Issue 18
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Original Articles

Reaction of Chlorosulfonyl Isocyanate With 1,2-Diols: Rearrangement and Formation of Carbonates

Sajan P. Joseph Department of Chemistry, Indian Institute of Technology, Kanpur, 208 016, INDIA
&
D. N. Dhar Department of Chemistry, Indian Institute of Technology, Kanpur, 208 016, INDIA
Pages 2295-2302 | Published online: 03 Jan 2007
 
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Abstract

1,2-Diols, 1a-e, upon reaction with chloro-sulfonyl isocyanate (CSI) gave the ketones, 3a-e Under similar experimental conditions, 1,2-diols, 1f-k, gave carbonyl compounds, 3f-k, carbonates, 6f-k, carboxamides, 7h, i, and the epoxide, 5i.

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