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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 1-2
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Original Articles

α-Lithioalkylphosphonates as Functional Group Carriers. Part II. A Direct (E)-Cinnamic And 2-Alkyl-Cinnamic Acids Synthesis

Marie-Paule Teulade Laboratoire de Chimie du Phosphore et des Métaux de Transition DCPH, Ecole Polytechnique, 91128, Palaiseau Cedex, France
,
Philippe Savignac Laboratoire de Chimie du Phosphore et des Métaux de Transition DCPH, Ecole Polytechnique, 91128, Palaiseau Cedex, France
,
Elie About-jaudet Laboratoire des Composés Organophosphorés, INSA-IRCOF, BP 08, 76131, Mont-Saint-Aignan, France
&
Noël Collignon Laboratoire des Composés Organophosphorés, INSA-IRCOF, BP 08, 76131, Mont-Saint-Aignan, France
Pages 71-81 | Received 01 Jun 1988, Published online: 24 Oct 2006
 
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Abstract

Sequential treatment of α-lithioalkylphosphonates with tert-butyl fluoroformate or di-tert-butyl dicarbonate and an aromatic aldehyde gives tert-butyl acrylic esters convertible into acrylic acids by protolysis with trifluoroacetic acid.

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