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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 1-2
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Original Articles

Generation and Michael Reaction of 1, 3-Bis(trimethylsiloxy)-isoindoles by Reduction of N-Alkylphthalimides with a Zn-Me3SiCl-Lutidine System

Tsutomu Inokuchi Department of Applied Chemistry, Faculty of Engineering, Okayama University, Tsushima, Okayama, 700, Japan
,
Hidetoshi Yamashita Department of Applied Chemistry, Faculty of Engineering, Okayama University, Tsushima, Okayama, 700, Japan
,
Takashi Date Department of Applied Chemistry, Faculty of Engineering, Okayama University, Tsushima, Okayama, 700, Japan
&
Sigeru Torii Department of Applied Chemistry, Faculty of Engineering, Okayama University, Tsushima, Okayama, 700, Japan
Pages 267-274 | Received 22 Mar 1988, Published online: 24 Oct 2006
 
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Abstract

Formation and concomitant Michael reaction of 1,3-bis(trimethylsiloxy)isoindoles have been achieved by the reduction of phthalimides with a Zn-Me3SiCl-lutidine system in the presence of α, β-unsaturated carbonyl compounds under sonication.

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