Improved Synthesis of 1-Chloroadamantane by Hydride Transfer Induced by Tertiarybutylchloride: Synthetic Communications: Vol 19, No 9-10

Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 19, 1989 - Issue 9-10

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Abstract

Adamantane was chlorinated, without chlorine, by tertiarybutylchloride and Lewis acids. The result with AlCl₃ gives the best yield (90.5%) and selectivity (95.4%) in 1-chloroadamantane so far reported. The results are consistent with an hydride transfer mechanism.

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Improved Synthesis of 1-Chloroadamantane by Hydride Transfer Induced by Tertiarybutylchloride

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Improved Synthesis of 1-Chloroadamantane by Hydride Transfer Induced by Tertiarybutylchloride

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