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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 13
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Original Articles

An Improved Procedure for Mono C-Alkylation of Pentane-2.4-Dione with ω-Bromoacid Esters

David P. Shrout Department of Chemistry, University of Nevada Reno, Nevada, 89557-0020
&
David A. Lightner Department of Chemistry, University of Nevada Reno, Nevada, 89557-0020
Pages 2075-2080 | Received 04 May 1990, Published online: 24 Oct 2006
 
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Abstract

Pentane-2,4-dione is alkylated by ethyl bromoacetate or ethyl 6-bromohexanoate in high yield in CH2C12 or 5:1 CH3CN-(CH3)2SO solvents, using one equivalent of K2CO3-Cs2CO3 as base.

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