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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 1
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Original Articles

A Procedure for the Oxidative “Dimerization” of Aliphatic 1-Alkynes

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Pages 137-139 | Received 21 Nov 1990, Published online: 24 Sep 2006
 

Abstract

Aliphatic 1-alkynes RC≡CH (R=alkyl) are readily converted into diynes RC≡CC≡CR, by introducing oxygen into a mixture of the acetylene and pyridine using copper(I)bromide as a catalyst and 1,8-diazabicyclo[5.4.0] undec-7-ene as a co-catalyst.

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