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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 15-16
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Original Articles

Cyclization of Chlorosulfonyl Isocyanate with Phenylhydrazones: A Synthetic Route to Triazinonoxathiazinedioxides and Triazinones

Joseph Daniel Department of Chemistry, Indian Institute of Technology, Kanpur, 208016, India
&
D. N. Dhar Department of Chemistry, Indian Institute of Technology, Kanpur, 208016, India
Pages 1695-1703 | Received 07 May 1991, Published online: 23 Sep 2006
 
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Abstract

A convenient synthetic route is reported for the preparation of aroyl substituted triazinones and triazinono-xathiazinedioxides by the interaction of chlorosulfonyl isocyanate and phenylhydrazones (derived from acetylacetone, 1-benzoylacetone and dibenzoylmethane).

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