Synthesis of 2-Hydroxy-3-methyl-2-cyclo-pentenone, Corylone, from 2-Ketoglutaric Acid: Synthetic Communications: Vol 21, No 17

Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 21, 1991 - Issue 17

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Abstract

Treatment of 2-ketoglutaric acid with diazomethane gave 2-(metoxycarbonyl)-oxiranepropanoic acid methyl ester (2) wich lead to 2-hydroxy-2-methyl-glutaric acid dimethyl ester (3) by catalytic hydrogenation, wich was further processed to the title compound.

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Synthesis of 2-Hydroxy-3-methyl-2-cyclo-pentenone, Corylone, from 2-Ketoglutaric Acid

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Synthesis of 2-Hydroxy-3-methyl-2-cyclo-pentenone, Corylone, from 2-Ketoglutaric Acid

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