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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 22
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Original Articles

Preparation of Enantiomerically Pure 1,3-Butanediol from Threonine

Marc Larchevêque UPR 402 du CNRS, Laboratoire de Chimie, Ecole Normale Supérieure, 24, rue Lhomond, 75231, Paris, Cedex, 05, France
,
Lengo Mambu UPR 402 du CNRS, Laboratoire de Chimie, Ecole Normale Supérieure, 24, rue Lhomond, 75231, Paris, Cedex, 05, France
&
Yves Petit UPR 402 du CNRS, Laboratoire de Chimie, Ecole Normale Supérieure, 24, rue Lhomond, 75231, Paris, Cedex, 05, France
Pages 2295-2300 | Received 24 Jun 1991, Published online: 23 Sep 2006
 
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Abstract

Enantiomerically pure R or S 1,3-butanediols were prepared in four steps from L or D threonine by nitrous deamination in the presence of bromide ion followed by esterification and reduction.

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