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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 22
70
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Original Articles

Preparation and Reaction of Cyclic Oxalate of Diols

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Pages 2361-2367 | Received 27 Jun 1991, Published online: 23 Sep 2006
 

Abstract

Cyclic oxalates were efficiently prepared by the reaction of diols with ethyl oxalyl chloride in the presence of triethylamine. They were stable under acidic conditions but cleaved to diols under basic conditions.

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