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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 15
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Original Articles

Palladium-Catalyzed Preparation of Dialkyl Allylphosphonates. A New Preparation of Diethyl 2-Oxoethylphosphonate

R. Malet Department of Chemistry, Universitat Autònoma de Barcelona, Bellaterra, 08193, Barcelona, Spain
,
M. Moreno-Mañas Department of Chemistry, Universitat Autònoma de Barcelona, Bellaterra, 08193, Barcelona, Spain
&
R. Pleixats Department of Chemistry, Universitat Autònoma de Barcelona, Bellaterra, 08193, Barcelona, Spain
Pages 2219-2228 | Received 02 Apr 1992, Published online: 24 Sep 2006
 
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Abstract

Palladium-catalyzed Michaelis-Arbuzov reaction of allyl acetates with trialkyl phosphites affords dialkyl allylphosphonates. Diethyl 2-oxoethylphosphonate is efficiently prepared by ozonization of diethyl allylphosphonate.

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