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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 7
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Original Articles

Convenient Synthesis of Vinyldiazomethanes from α-Diazo-β-Keto Esters and Related Systems

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Pages 971-978 | Received 14 Oct 1991, Published online: 24 Sep 2006
 

Abstract

A series of vinydiazomethanes were readily prepared by sodium borohydride reduction of a-diazo-p-ketoesters followed by phosphorus oxychloride induced dehydration of the resulting a-diazo-p-hydroxyesters.

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