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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 20
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Original Articles

Convenient Conversion of cis-Homoallylic Alcohols into Corresponding Bromides with Ph3PBr2

Jacqueline Sandri Laboratoire de Synthèse Organique Associé au CNRS, URA 1411, Université d'Aix-Marseille III-F, 13397, Marseille Cedex 13
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Jacques Viala Laboratoire de Synthèse Organique Associé au CNRS, URA 1411, Université d'Aix-Marseille III-F, 13397, Marseille Cedex 13
Pages 2945-2948 | Received 04 Jun 1992, Published online: 23 Sep 2006
 
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Abstract

An mild and easy worked up procedure using the cheap reagent Ph3PBr2 allowed us to improve the conversion of sensitive alcohols (homoallylic and acetalized) into their corresponding bromides in high yields.

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