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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 5
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Original Articles

Regioselective Acylation of Benzoselenazolinone

V. Galet Institut de Chimie Pharmaceutique, 3 rue du Professeur Laguesse, BP 83 F, 5906, Lille Cedex
,
M. P. Vaccher Institut de Chimie Pharmaceutique, 3 rue du Professeur Laguesse, BP 83 F, 5906, Lille Cedex
,
J. L. Bernier I.N.S.E.R.M. U 16, place de Verdun, F - 59045, Lille Cedex
,
J. P. Henichart I.N.S.E.R.M. U 16, place de Verdun, F - 59045, Lille Cedex
&
D. Lesieur Institut de Chimie Pharmaceutique, 3 rue du Professeur Laguesse, BP 83 F, 5906, Lille Cedex
Pages 621-629 | Received 11 Sep 1992, Published online: 27 Oct 2006
 
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Abstract

Substitutions on benzoselenazolinone were performed by using successively (i) aliphatic or aromatic acids and (ii) acid chlorides in the presence of (i) polyphosphoric acid and (ii) aluminium chloride in dimethylformamide. Regioselective acylation at C6 position was demonstrated by 1H NMR using Nuclear Overhauser Effect.

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