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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 5
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Original Articles

Triphosgene/Triphenylphosphine: A Mild Reagent for the Conversion of Alcohols to Chlorides

I. A. Rivero Centro de Graduados e Investigacion del Instituto Tecnológico de Tijuana, Apdo. Postal 1166, 22000, Tijuana, B. C., Mexico
,
R. Somanathan Centro de Graduados e Investigacion del Instituto Tecnológico de Tijuana, Apdo. Postal 1166, 22000, Tijuana, B. C., Mexico
&
L. H. Hellberg Centro de Graduados e Investigacion del Instituto Tecnológico de Tijuana, Apdo. Postal 1166, 22000, Tijuana, B. C., Mexico
Pages 711-714 | Received 23 Sep 1992, Published online: 27 Oct 2006
 
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Abstract

A mixture of triphosgene/triphenylphosphine in methylene chloride converts primary and secondary alcohols to chlorides at room temperature.

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