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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 14
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Original Articles

A New, Convenient and Efficient Procedure for the Synthesis of Phosphodiesters Using Chloro N,N-Diisopropylaminoalkyloxyphosphines

Yang Lu Ecole Nationnale Supérieure de Chimie de Paris, Laboratoire de Bioorganique et Biotechnologies (URA 1389 CNRS) 11, rue Pierre et Marie Curie, 75231, Paris CEDEX, 05, FRANCE
&
François Le Goffic Ecole Nationnale Supérieure de Chimie de Paris, Laboratoire de Bioorganique et Biotechnologies (URA 1389 CNRS) 11, rue Pierre et Marie Curie, 75231, Paris CEDEX, 05, FRANCE
Pages 1943-1946 | Received 22 Feb 1993, Published online: 16 Feb 2007
 
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Abstract

A general procedure is described for the preparation of phosphodiesters by treating alcohols with chloro-N,N-diisopropylaminoalkyloxyphosphines I in the presence of pyridine followed by mild oxidation.

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