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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 23, 1993 - Issue 9
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Original Articles

Preparation of Dichloroacetaldehyde Cyclic Trimer and Its Depolymerization

Takashi Wakasugi Kureha Chemical Industry Co., Ltd. Nishiki Plant Nishiki-machi, Iwaki, 974, JAPAN
,
Tadashi Miyakawa Kureha Chemical Industry Co., Ltd. Nishiki Plant Nishiki-machi, Iwaki, 974, JAPAN
,
Fukuichi Suzuki Kureha Chemical Industry Co., Ltd. Nishiki Plant Nishiki-machi, Iwaki, 974, JAPAN
,
Shinichi Itsuno Kureha Chemical Industry Co., Ltd. Nishiki Plant Nishiki-machi, Iwaki, 974, JAPAN; Department of Materials Science, Toyohashi University of Technology, Tempaku-cho, Toyohashi, 441, JAPAN
&
Koichi Ito Kureha Chemical Industry Co., Ltd. Nishiki Plant Nishiki-machi, Iwaki, 974, JAPAN; Department of Materials Science, Toyohashi University of Technology, Tempaku-cho, Toyohashi, 441, JAPAN
Pages 1289-1294 | Received 04 Aug 1992, Published online: 24 Sep 2006
 
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Abstract

Dichlorination of paraldehyde followed by hydration gave white crystals of dichloroacetaldehyde(DCA) hydrate which were treated with concd sulfuric acid at 0 °C to afford a cyclic trimer of DCA as a quite stable precursor of DCA.

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