Electrooxidation of Thiols in the Presence of Halide Ions—A Facile Preparative Method for Synthesis of Disulfides

M. E. Niyazymbetov N.D.Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Leninsky Prospekt 47, 117913, Moscow, Russian Federation

L. D. Konyushkin N.D.Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Leninsky Prospekt 47, 117913, Moscow, Russian Federation

Z. I. Niyazymbetova N.D.Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Leninsky Prospekt 47, 117913, Moscow, Russian Federation

V. P. Litvinov N.D.Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Leninsky Prospekt 47, 117913, Moscow, Russian Federation

V. A. Petrosyan N.D.Zelinsky Institute of Organic Chemistry Russian Academy of Sciences, Leninsky Prospekt 47, 117913, Moscow, Russian Federation

Abstract

The aliphatic, aromatic and heteroaromatic disulfides were easily synthesized by the electrolysis of corresponding thiols. The electrochemical method is also convenient for synthesis of unsymmetrically substituted disulfides and “paired” synthesis of disulfide and sulfide.

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Electrooxidation of Thiols in the Presence of Halide Ions—A Facile Preparative Method for Synthesis of Disulfides

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Electrooxidation of Thiols in the Presence of Halide Ions—A Facile Preparative Method for Synthesis of Disulfides

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