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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 11
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Original Articles

A Facile New Synthesis of Aldehyde Enamines in High Yield and High Purity

Gary B. Fisher Department of Chemistry and Biochemistry, University of California, Santa Cruz, Santa Cruz, CA, 95064
,
Lawrence Lee Department of Chemistry and Biochemistry, University of California, Santa Cruz, Santa Cruz, CA, 95064
&
Frederick W. Klettke Department of Chemistry and Biochemistry, University of California, Santa Cruz, Santa Cruz, CA, 95064
Pages 1541-1546 | Received 09 Sep 1993, Published online: 23 Sep 2006
 
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Abstract

Aldehyde enamines were synthesized in excellent yield and purity by reacting an aldehyde with 2 equivalents of a secondary amine in cyclohexane in the presence of 1.5 equivalents of CaH2. Distilled yields ranged from 65%-92%.

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