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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 16
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Original Articles

A Mild and Efficient Detritylation of Some Carbohydrate Derivatives

J. Fuentes Departamento de Química Orgánica. Facultad de Química, Universidad de Sevilla, 41071, Seville, Spain
,
T. Cuevas Departamento de Química Orgánica. Facultad de Química, Universidad de Sevilla, 41071, Seville, Spain
&
M. A. Pradera Departamento de Química Orgánica. Facultad de Química, Universidad de Sevilla, 41071, Seville, Spain
Pages 2237-2245 | Received 31 Jan 1994, Published online: 23 Sep 2006
 
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Abstract

Solutions of Cl2 in CHCl3 are used to remove the trityl radical from CH2OTr groups of carbohydrate derivatives. This method does not produce cleavage of the C-N bond in nucleosides. An N-dialkoxy-carbonylvinyl group can be simultaneously removed.

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