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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 24, 1994 - Issue 16
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Original Articles

Reaction of Pummerer Rearrangement Intermediate with Thiols: New Synthetic Method of S,S-Thioacetals of Formylphosphonate

Taek Hyeon Kim Department of Fine Chemical Technology, Chonnam National University, Kwangju, 500-757, Korea
&
Dong Young Oh Department of Chemistry, Korea Advanced Institute of Science and Technology, Taejeon, 305-701, Korea
Pages 2313-2318 | Received 07 Dec 1993, Published online: 23 Sep 2006
 
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Abstract

Pummerer rearrangement reaction intermediate(2) of phenylsulfinyl methanephosphonate(1) has been found to react mildly with thiols(3) in the presence of stannic chloride to provide S,S-thioacetals of formylphosphonate(4).

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