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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 23
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Original Articles

Some Observations on Baeyer-Villiger Oxidation of Alicyclic Ketones with Magnesium Monoperoxyphthalte in Aprotic Solvent in the Presence of Bentonite Clay

Masao Hirano Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, JAPAN
,
Yosimitsu Ueno Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, JAPAN
&
Takashi Morimoto Department of Applied Chemistry, Faculty of Technology, Tokyo University of Agriculture and Technology, Koganei, Tokyo, 184, JAPAN
Pages 3765-3775 | Received 19 Apr 1995, Published online: 23 Sep 2006
 
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Abstract

Magnesium monoperoxyphthalate oxidation of unsubstituted and substituted cyclohexanones has been carried out in acetonitrile in the presence of bentonite clay, affording the corresponding ε-caprolactones in fairly good yields.

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