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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 23
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Original Articles

A New Route to Monoalkylhydrazines

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Pages 3805-3812 | Received 11 Apr 1995, Published online: 23 Sep 2006
 

Abstract

Electrophilic amination of primary amines with N-(dietho-xyphosphoroyl)-O-(p-nitrophenylsulfonyl)-hydroxylamine 1, followed by dephosphorylation of the phosphorohydrazidate 2 with p-toluenesulfonic acid monohydrate in ethanol, represents a novel approach to monoalkylhydrazines.

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