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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 23
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Original Articles

Preparation of Functionalized α-Chloromethyl Ketones Using Rieke Zinc

Reuben D. Rieke Department of Chemistry, University of Nebraska-Lincoln, Lincoln, Nebraska, 68588-0304
,
Jeff D. Brown Department of Chemistry, University of Nebraska-Lincoln, Lincoln, Nebraska, 68588-0304
&
Xiaoming Wu Department of Chemistry, University of Nebraska-Lincoln, Lincoln, Nebraska, 68588-0304
Pages 3923-3930 | Received 07 May 1995, Published online: 23 Sep 2006
 
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Abstract

The cross-coupling reaction of highly functionalized organozinc reagents with chloroacetyl chloride mediated by copper allows for the easy preparation of functonalized α-chloromethyl ketones in excellent yields.

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