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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 24
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Original Articles

A Simple Procedure for Selective Acylation of the Less Reactive Hydroxyl Functionality in Some Dihydroxylated Compounds

Emil Pop Pharmos Corporation, 2 Innovation Drive, Alachua, FL, 32615
,
Ferenc Soti Pharmos Corporation, 2 Innovation Drive, Alachua, FL, 32615
&
Marcus E. Brewster Pharmos Corporation, 2 Innovation Drive, Alachua, FL, 32615
Pages 4099-4106 | Received 20 May 1995, Published online: 23 Sep 2006
 
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Abstract

Phenolic (3′) esters (acetate, N-t-Boc glycinate) of the (+) 3S, 4S 5′(1′,1′-dimethylheptyl)-7-hydroxy-δ6−tetrahydrocannabinol (dexanabinol) were synthesized via the 7′-trifluoroacetate followed by acylation and subsequent deprotection.

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