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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 25, 1995 - Issue 15
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Original Articles

Potassium Fluoride on Alumina: One-Pot Synthesis of Allyl Dithioesters by Tandem Condensation- Alkylation-Sigmatropic Rearrangement

Didier Villemin Ecole Nationale Supérieure d'h; Ingénieurs de Caen, I.S.M.R.A., Groupe Catalyse et Modélisation (U.R.A. 480), F-14050, Caen, Cedex, France Fax: E-mail: [email protected]
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Messaoud Hachemi Ecole Nationale Supérieure d'h; Ingénieurs de Caen, I.S.M.R.A., Groupe Catalyse et Modélisation (U.R.A. 480), F-14050, Caen, Cedex, France Fax: E-mail: [email protected]
Pages 2305-2310 | Received 09 Nov 1994, Published online: 23 Sep 2006
 
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Abstract

Methylene ketones adsorbed on KF-alumina at room temperature react quickly with carbon disulfide and two equivalents of allyl chloride. The products undergo sigmatropic rearrangement, to give the corresponding allyl ketodithioesters.

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