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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 8
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Original Articles

Preparation of Substituted Vinylsilanes from Cinnamyl Carbamates

Paul H. Mason Department of Chemistry, University of Natal, Private Bag X01, Scottsville, 3209, Republic of South Africa
&
Neville D. Emslie Department of Chemistry, University of Natal, Private Bag X01, Scottsville, 3209, Republic of South Africa
Pages 1473-1483 | Received 29 Sep 1995, Published online: 15 Aug 2006
 
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Abstract

Reaction of N,N-diethyl cinnamyl carbamate with TBDMSC1 yields the mono-silylated carbamate which, on treatment with butyllithium, reacts with various electrophiles to give the corresponding disubstituted carbamates.

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