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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 8
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Original Articles

Synthesis of 2,7-Diazabicyclo[3.3.0]octane and 2,7-Diazabicyclo[3.3.0]oct-4-ene Derivatives via Cyclization Reaction and Julia Reaction

Jae Wook Lee R&D Center, Dae Woong Pharmaceutical Co., LTD, 223-23 Sangdaewondong Sungnam, 462-120, Korea
,
Ho Jung Son R&D Center, Dae Woong Pharmaceutical Co., LTD, 223-23 Sangdaewondong Sungnam, 462-120, Korea
,
Yeon Eui Jung R&D Center, Dae Woong Pharmaceutical Co., LTD, 223-23 Sangdaewondong Sungnam, 462-120, Korea
&
Jae Ho Lee R&D Center, Dae Woong Pharmaceutical Co., LTD, 223-23 Sangdaewondong Sungnam, 462-120, Korea
Pages 1499-1505 | Received 02 Oct 1995, Published online: 15 Aug 2006
 
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Abstract

2,7-Diazabicyclo[3.3.0]octan-4-ol (1) and 2,7-diazabicyclo[3.3.0]oct-4-ene (2) are synthesized by the desulfonylation using Mg-HgCl2(cat.) of β-hydroxy sulfone derivatives which have been prepared via cyclization of sulfone ester derivative.

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