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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 3
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Original Articles

An Improved Procedure for the Synthesis of Chiral 2-Aza-Bicyclo[2.2.1]heptane

Charles K.F. Chiu Pfizer Inc. Central Research, Department of Process R&D, Eastern Point Road, Groton, Connecticut, 06340, U.S.A.
Pages 577-584 | Received 13 Jul 1995, Published online: 21 Aug 2006
 
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Abstract

Grieco's protocol for the synthesis of 2-aza-bicyclo[2.2.1]heptane is modified and adapted for large scale preparation. The optical purity of the material is readily upgraded by purification through a chiral salt.

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