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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 18
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Original Articles

Thermal Cleavage of Oxazolidine-4,5-diones to Imines: A Short Synthesis of 3,4-Dihydro-3,3-dimethyl-7-trifluoromethylisoquinoline-2-oxide

Ronald C. Bernotas Hoechst Marion Roussel, 2110 E. Galbraith Road, Cincinnati, OH, 45215
,
Ginette Adams Hoechst Marion Roussel, 2110 E. Galbraith Road, Cincinnati, OH, 45215
&
Thaddeus R. Nieduzak Hoechst Marion Roussel, 2110 E. Galbraith Road, Cincinnati, OH, 45215
Pages 3471-3477 | Received 14 Apr 1996, Published online: 21 Aug 2006
 
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Abstract

A series of oxazolidine-4,5-diones 2 was thermally cleaved to cyclic imines 3 in excellent yield. This reaction was utilized in an efficient synthesis of a 3,4-dihydroisoquinoline-based nitrone 1b.

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