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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 21
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Original Articles

(±)-3,4,4a,5,6,7-Hexahydro-4a-Methyl-7,7-Diphenyl-1(2H)-Naphthtlenone

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Pages 4081-4089 | Published online: 23 Aug 2006
 

Abstract

The title compound was prepared in 48% overall yield using a seven-step sequence. The synthesis involves stepwise construction of a 3-formyl-3,3-diphenypropyl side chain from the double bond of 3-ethenyl-3-methylcyclohexanone followed by aldol ring closure. The approach represents a general strategy for the synthesis of a number of (±)-7,7-diary1–3,4,4a,5,6,7-hexahydro-1(2H)-naphthalenones.

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