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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 1
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Original Articles

Facile Bromination of O-Benzylidene Sugar and THP Ethers with NBS in Chloroform in the Presence of AIBN

Sushil Raina Department of Chemistry, Indian Institute of Technology, Kanpur, India, 208 016
,
Kamal K. Srivastava Department of Chemistry, Indian Institute of Technology, Kanpur, India, 208 016
,
E. Sampath Kumar Department of Chemistry, Indian Institute of Technology, Kanpur, India, 208 016
&
Vinod K. Singh Department of Chemistry, Indian Institute of Technology, Kanpur, India, 208 016
Pages 121-125 | Received 16 May 1995, Published online: 21 Aug 2006
 
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Abstract

N-Bromosuccinimide in chloroform in the presence of a catalytic amount of AIBN is found to cleave O-benzylidene sugar into bromobenzoate in efficient manner. THP-ethers were cleaved into bromides and bromo-esters in high yield.

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