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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 13
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Original Articles

On A Safe and Practical Method for The Preparation of β-Keto Phosphonates1

Bernard Corbel Laboratoire de Chimie Hétéro-Organique, U.F.R. Sciences, B.P. 809, F-29285, Brest Cedex
,
Isabelle L'Hostis-Kervella Laboratoire de Chimie Hétéro-Organique, U.F.R. Sciences, B.P. 809, F-29285, Brest Cedex
&
Jean-Pierre Haelters Laboratoire de Chimie Hétéro-Organique, U.F.R. Sciences, B.P. 809, F-29285, Brest Cedex
Pages 2561-2568 | Received 15 Jan 1996, Published online: 23 Aug 2006
 
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Abstract

Acylations of the magnesium enolate derivatives of trimethyl and triethylphosphonoacetates, using a magnesium chloride-triethylamine system, lead to 2-acylphosphonoacetates which are decarbalkoxylated to give β-keto phosphonates.

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