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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 14
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Original Articles

The Synthesis of D,L-15-Acetoxypallescensin-A: An Intramolecular Oxidative Free-Radical Approach

Phillip A. Zoretic Department of Chemistry, East Carolina University, Greenville, North Carolina, 27858
&
Ming Wang Department of Chemistry, East Carolina University, Greenville, North Carolina, 27858
Pages 2783-2796 | Received 02 Feb 1996, Published online: 21 Aug 2006
 
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Abstract

The synthesis of d,l-15-acetoxypallescensin-A 3 is reported. An intramolecular oxidative radical cyclization was used as a stereoselective entry to trans-decalin 12 which was converted in two steps to the pallescensin-A skeleton 14 by modification of Hagiwara's furan procedure.

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