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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 22
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Original Articles

Zinc Promoted Addition of Methyl 2,2-Dihalocarboxylates to Carbonyl Compounds

Marta Benincasa Dipartimento di Chimica, dell' Università, Via Campi 183, I-41100, Modena, (Italy)
,
Luca Forti Dipartimento di Chimica, dell' Università, Via Campi 183, I-41100, Modena, (Italy)
,
Franco Ghelfi Dipartimento di Chimica, dell' Università, Via Campi 183, I-41100, Modena, (Italy)
,
Emanuela Libertini Dipartimento di Chimica, dell' Università, Via Campi 183, I-41100, Modena, (Italy)
&
Ugo M. Pagnoni Dipartimento di Chimica, dell' Università, Via Campi 183, I-41100, Modena, (Italy)
Pages 4113-4122 | Received 04 Jun 1996, Published online: 19 Aug 2006
 
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Abstract

Methyl 2,2-dihalocarboxylates add easily to carbonyl compounds in fair to good yields through the intermediate formation of 2-haloester enolates; the reaction is promoted by zinc, following a “Barbier” type procedure.

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