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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 26, 1996 - Issue 15
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Original Articles

Influence of an Oxidising Impurity on Preparation of 2-Lithio-1,3-dithiane: Isolation of bis[2-d,3-Dithianyl)]methanol

Narshinha P. Argade Division of Organic Chemistry Synthesis, National Chemical Laboratory, Pune, 411 008, India
,
Braja G. Hazra Division of Organic Chemistry Synthesis, National Chemical Laboratory, Pune, 411 008, India
&
Padmakar L. Joshi Division of Organic Chemistry Synthesis, National Chemical Laboratory, Pune, 411 008, India
Pages 2797-2802 | Received 10 Jan 1996, Published online: 21 Aug 2006
 
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Abstract

Bis-dithianylalkanols and dimers are formed in preparation of 2-lithio-1,3-dithianes due to the presence of oxidising impurity in n-BuLi (perhaps n-BuOOLi).

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