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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 6
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Original Articles

Preparation of Disulfides by Reduction of Sodium Alkyl Thiosulfates with Metallic Samarium and Catalytic Amount of Iodine

, &
Pages 1043-1047 | Received 12 Aug 1996, Published online: 22 Aug 2006
 

Abstract

Sm/I2 reduces sodium alkyl thiosulfates to the corresponding disulfides in good to excellent yields in THF at room temperature.

Notes

b. ibid. pp 466

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