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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 16
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Original Articles

Preparation of Protected Serinol

Karsten Sorbye Department of Chemistry Norwegian, University of Science and Technology, NTNU N-7034, Trondheim, Norway E-mail: E-Mail: [email protected]
&
Per H.J. Carlsen Department of Chemistry Norwegian, University of Science and Technology, NTNU N-7034, Trondheim, Norway E-mail: E-Mail: [email protected]
Pages 2813-2816 | Received 27 Mar 1997, Published online: 22 Aug 2006
 
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Abstract

. An effective procedure for the preparation of the benzylidene protected serinol, 5-amino-2-phenyl-1,3-dioxane, is described. Catalytic reductive amination of O,O'-benzylidene dihydroxyacetene, BDHA, with ammonia in anhydrous ethanol gave the pure product in high yield.

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