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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 16
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Original Articles

Synthesis of (Trifluoromethylthio) Cubanes

S. Munavalli Geo-Centers, Inc., Ft., Washington, MD, 20744, Geo-Centers, Inc.
,
G. W. Wagner Geo-Centers, Inc., Ft., Washington, MD, 20744, Geo-Centers, Inc.
,
A. Bashir Hashemi Lake Hopatcong, NJ, 07849
,
D. K. Rohrbaugh U. S. Army, Edgewood Research Development and Engineering Center, Aberdeeen Proving Ground, MD, 21010
&
H. D. Durst U. S. Army, Edgewood Research Development and Engineering Center, Aberdeeen Proving Ground, MD, 21010
Pages 2847-2851 | Received 27 Mar 1997, Published online: 22 Aug 2006
 
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Abstract

Reaction of trifluoromethylthiocopper with 1,4-diiodo- and 1-bromo-4-iodocubanes furnishes 1-iodo-4-(trifluoromethylthio)-, 1-bromo-4-(trifluoromethylthio)- and 1,4-bis(trifluoromethylthio)cubanes in respectable yields.

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