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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 18
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Original Articles

The HSnPh3 Free Radical Mediated Cyclization of 4,9-Dioxa-1,6-dodecadien-11-yne

Pages 3163-3170 | Received 17 Feb 1977, Published online: 22 Aug 2006
 

Abstract

We report the triphenyltin hydride radical mediated cyclization of 4,9-dioxa-1,6-dodecadien-11-yne 2. The reaction proceeds under very mild conditions and in good chemical yield (59%), giving a mixture of products 5 (mixture of isomers in a 1:2 ratio) and 6 (mixture of isomers in a 1:3 ratio).

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