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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 1
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Original Articles

Syntheses of 9,10-Phenanthrenequinone and 9-Methoxyphenanthrene by Oxidation of Phenanthrene with Dihydroxy Phenylselenonium Benzenesulfonate

Nicolai Stuhr-Hansen Department of Chemistry, University of Copenhagen, Universitetsparken 5, DK-2100, Copenhagen Ø, Denmark
&
Lars Henriksen Department of Chemistry, University of Copenhagen, Universitetsparken 5, DK-2100, Copenhagen Ø, Denmark
Pages 89-94 | Received 25 Jun 1996, Published online: 19 Aug 2006
 
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Abstract

9,10-Phenanthrenequinone is prepared by oxidation of phenanthrene with dihydroxy phenylselenonium benzenesulfonate in boiling dioxane-water. 9-methoxyphenanthrene is obtained when the reaction is carried out in methanol.

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