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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 22
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Original Articles

Tributyltin Hydride-Induced Free Radical Deoxygenation of the Cyclic Thionocarbonates of Threo-2,3-Dihydroxy Esters and Ketones

Pages 3887-3893 | Received 14 Apr 1997, Published online: 22 Aug 2006
 

Abstract

Abstract: A practical and enantiospecific method for the synthesis of optically pure β-hydroxy esters and ketones is described. The key reaction is free radical deoxygenation of the cyclic thionocarbonates of threo-2,3-dihydroxy esters and ketones with tributyltin hydride.

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