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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 27, 1997 - Issue 22
45
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Original Articles

Synthesis of 5α-Iodo-6-one Steroids

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Pages 3997-4002 | Received 17 Jun 1997, Published online: 22 Aug 2006
 

Abstract

Abstract: The synthesis of 5-iodo-5α-cholestan-6-one (6), its 3β-acetoxy-(7) and 3β-chloro-(8) analogues, 3β-acetoxy-5-iodo-5α-stigmastan-6-one (9) and its 3β-chloro-(10) analogue by the reacion of silver chromate-iodine and pyridine with the corresponding steroidal olefins (1-5) is described. The structures of these products have been established on the basis of their elemental, analytical and spectral data.

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