Phase Transfer Catalyzed Synthesis of 1,6-Diaroyldithiohydrazodicarbonamide Derivatives

Youming Zhang Department of Chemistry, Northwest Normal University, Lanzhou, Gansu, 730070, China

Taibao Wei Department of Chemistry, Northwest Normal University, Lanzhou, Gansu, 730070, China

Jinren Lu Department of Chemistry, Northwest Normal University, Lanzhou, Gansu, 730070, China

Abstract

Reaction of hydrazine hydrate with aroyl chloride and ammonium thiocyanate under the condition of solid-liquid phase transfer catalysis using polyethylene glycol-600 (PEG-600) as the catalyst yielded 1, 6-diaroyldithiohydrazodicarbonamides 3a—3h in good to excellent yield.

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Phase Transfer Catalyzed Synthesis of 1,6-Diaroyldithiohydrazodicarbonamide Derivatives

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Phase Transfer Catalyzed Synthesis of 1,6-Diaroyldithiohydrazodicarbonamide Derivatives

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