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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 17
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Original Articles

Novel Reductive Dimerization Cyclization of 1,1-Dicyanoalkenes Mediated by Zinc in Aqueous Media

Lei Wang Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
&
Yongmin Zhang Department of Chemistry, Hangzhou University, Hangzhou, 310028, P. R. China
Pages 3269-3277 | Received 11 Mar 1998, Published online: 23 Aug 2006
 
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Abstract

Zinc-mediated reductive dimerization cyclization of 1,1-dicyanoalkenes 1 occurs to give functionalized cyclopentenes 2(cis) and 3(trans) in good yields under saturated aqueous NH4Cl-THF solution at room temperature. 3 is major product.

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